By Michael Dub (auth.), Michael Dub (eds.)

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Extra info for Compounds of Arsenic, Antimony, and Bismuth: Covering the Literature from 1965 to 1968

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From [Pd2(trans-o-H2NCa~SCH2CH=CHCH2SCa~NH2-o)C~] + Ars in EtOH at 20°. IR spectrum (628). [Pt(Ars)4J, rxn. with HCl in CeHe or EtOH - [HPt(ArS)2Cl] (298, 299). [HPt(ArS)2Cl] (M-25), white needles, m. 187-190° (109), m. 296-297° (298, 299), prepd. from [Pt(Ars)4] in CeHe + MeOH-HCl on a steam bath (109) and from [Pt(ArS)4] + HCl in CeHe or EtOH. A nonelectrolyte in PhN02 (298, 299). IR spectrum (109, 298, 299). cis-[Pt(Ars)2C12] (M-25), prepd. from [Pt2(trans-o-H2NCa~SCH2CH=CHCH2SCa~­ NH2-o)C~J + Ars in EtOH by heating under reflux.

Formed a yellow-orange soln. in CeRe and C~C12 and greenish yellow in CHCIs; stable in soln. and in the solid state, prepd. from [Rh(Ars)3Cl] by dissolving in C~C12 satd. with Hand concg. in a H atm. lR and NMR spectra; a cis coordination of both H atoms postulated. An octahedral configuration with the sixth position filled with a molecule of C~C12 was suggested. The complex is unable to transfer the H ligand to olefins. Addn. of Ph3P to the complex in CHCIs soln. gives mixed species (1006). [RhD(Ars)2(CO)C12], prepd.

Trixylylarsine, AsC24H27 Use: A stabilizer for photochromic systems such as mixts. of 2,3-diphenylindenone 2,3-epoxide and poly(methyl methacrylate) against mol. degradation (1544). : From AsC1 3 in Et20 by adding to a soln. , 21% yield (1519). : m. 240-242° (1519). Rxn. with: Pb(OAc)4 or with N/20 AgCl04 soln. in CeHe ~ a green colored radical cation (1519). : {Ir[As(Ce~NMe2-4)s](COD)Cl}*, m. > 1&J0, a monomer, nonconducting in ClCH2CH2Cl, prepd. from [Ir(COD)Cl]2 and the arsine (1:2). IR spectrum indicated the presence of both olefinic bonds coordinated with the metal atom.

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