By Robert Léon Wagner
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1980, 181, 108. J . Finne, T. Krusius, and H. Rauvala, Carbohydr. , 1980,80, 336. General Met h o ds 19 methylsulphenyl carbanion is necessary for the complete methylation of saccharides. 119 This can be demonstrated by the addition of triphenylmethane, which forms a red colour in the presence of the carbanion. Methylation of bacterial lipopolysaccharides has been accomplished using methyl trifluoromethane sulphonate in trimethylphosphate as a solvent. 120 The determination of the sugar sequence and glycosidic bond arrangement of heteroglycans by an integrated analytical scheme, which includes methylation analysis, periodate oxidation, acetolysis, and 0-elimination, has been proposed.
1980, 66, 870. C. A. Adams, R. W. Rinne, and M. C. Fjerstad, Ann. Bot. (London), 1980, 45, 577. Y . Watanabe, F. Ohta, and Y . Ayano, Agric. Biol. Chem. ), 1979, 43, 2625. D. A. McCracken and W. M. Rutherford, Anal. , 1980, 101, 275. G . N. Umezurike and S. A. Ekhorutomwen, Biochim. Biophys. Acta, 1979,567, 3 3 1 . Plant and Algal Polysaccharides 27 from the amylose extender ( a e ) Since no branching enzyme is present, the citrate-stimulated reaction could be characterized. Malate could be used instead of citrate and added branching enzyme increased the velocity 4-fold but did not replace the requirement for citrate.
L. , 1980, 57, 390. J . R. , 1980, 57,406. Zegota, J. , 1980, 192,446. H. C. Jarrell, T. F. Conway, P. Moyna, and I. C. P. Smith, Carbohydv. , 1979, 76,45. M. Buffa, G. Gongiu, A. Lombard, and M. L. Tourn, J. , 1980, 200, 309. Shiomi, J . Yamada, and M. Izawa,Agric. Biol. Chem. ), 1979, 43, 2233. Plant and Algal Polysaccharides 29 [ p-D-Fruf-(2 --* l)],-p-D-Fruf-(2 -+ 6)-au-D-Glcp-( 1 -+ 2)-p-D-Fruf (4) n = 0 ; (5) ~1 = 1; ( 6 ) n = 2 [p-D-Fruf-(:! 3 l)Im-p-D-Fruf-(2* 1)-a-D-Glcp 6 t 2 [p-D-Fruf-(2 +.